부산대학교 도서관

SiC (SCS-6TM) continuous fibre/SiC composites were fabricated by hot-pressing at 1700°C in vacuum using an Al sintering additive. Analytical transmission electron microscopy was used to investigate the microstructure of the composites. The room-temperature mechanical and high-temperature creep properties of the composites were investigated by four-point bending. The SiC powders used were sintered at a relatively low sintering temperature to high density (97% of theoretical density) with the addition of the Al sintering additive. It is believed that the Al additive is very efficient for the densification of SiC. The SiC fibres maintained their original form and microstructure during fabrication. The SiC matrix reacted with the outermost carbon sublayer in the fibre, forming a thin (1.8–4.8μm) interfacial layer, which was composed of Al4C3, Si–Al–C, and Si–Al–O phases. The incorporation of SiC fibre into a dense SiC matrix significantly increased the room-temperature failure strain and improved the high-temperature creep properties. In addition, the incorporation of SiC fibre into a porous SiC matrix increased the room-temperature failure strain, but did not contribute to the high-temperature creep properties.