학술논문

Synthesis of a naphthalene-hydroxynaphthalene polymer model compound
Document Type
Technical Report
Author
Source
Subject
01 COAL, LIGNITE, AND PEAT
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY COAL
COMBUSTION
ORGANIC COMPOUNDS
SYNTHESIS
PROGRESS REPORT
CARBONACEOUS MATERIALS
CHEMICAL REACTIONS
DOCUMENT TYPES
ENERGY SOURCES
FOSSIL FUELS
FUELS
MATERIALS
OXIDATION
THERMOCHEMICAL PROCESSES 014000* -- Coal, Lignite, & Peat-- Combustion
400201 -- Chemical & Physicochemical Properties
Language
English
Abstract
The objective of this project is the synthesis of a new naphthalene-hydroxynaphthalene polymer model compound for use in coal combustion studies. Since this compound is an unreported compound, this effort also requires the development of a synthetic route to this compound, including the synthesis of unreported intermediates leading to its synthesis. Complex product mixtures have been consistently obtained with all of our approaches. As a result, we have been constantly making small modifications to our technical approach. These changes are discussed in this report. Our synthesis efforts resulted in a number of potential precursors and intermediates. When appropriate, these compounds were submitted to the Organic Chemistry Research Area's Analytical Section for characterization and identification.