학술논문

Effect of calcination temperature on the electrospun MFe2O4 (M=Ni0.25-Cu0.25-Zn0.5)
Document Type
Conference
Source
2010 3rd International Nanoelectronics Conference (INEC) Nanoelectronics Conference (INEC), 2010 3rd International. :421-422 Jan, 2010
Subject
Components, Circuits, Devices and Systems
Computing and Processing
Engineered Materials, Dielectrics and Plasmas
Calcination
Temperature
Ferrites
X-ray scattering
Morphology
Magnetic materials
Lattices
Image storage
Material storage
Magnetic separation
Language
ISSN
2159-3523
2159-3531
Abstract
Nanoelectrospun fibers of MFe 2 O 4 (M = Ni 0.25 -Cu 0.25 -Zn 0.5 ) were fabricated by electrospinning technique using PVP solution and and metal nitrate as starting materials. The as spun fibers were calcined at different temperatures of 500, 600, 700 and 800 °C. The results from XRD indicated that the calcined nanofibers structure was face center cubic (fcc) with the lattice constant a = 0.83976±0.00028 nm. SEM micrograph showed as-spun nanofibers with the average diameter of 480±70 nm and the morphology of the nanofibers was changed to be more rough and wriggly after the calcinations with the diameters of 75–210 nm.