학술논문
固相萃取结合高效液相色谱测定鸡肉中10种磺胺类药物残留 / Simultaneous determination of sulfonamide residues in chicken muscle by solid phase ex-traction and high performance liquid chromatography
Document Type
Academic Journal
Author
Source
中国卫生检验杂志 / CHINESE JOURNAL OF HEALTH LABORATORY TECHNOLOGY. 18(11):2201-2203
Subject
Language
Chinese
ISSN
1004-8685
Abstract
目的:建立鸡肉中10种磺胺类药物残留的HPLC测定方法.方法:鸡肉经过甲醇提取,正己烷脱脂,SLW固相萃取柱净化,用HPLC法测定鸡肉中10种磺胺类药物的含量.结果:当鸡肉样品添加10种磺胺类药物为0.05～0.2 mg/kg时,方法回收率为67.4%～95.6%,变异系数为4.8%～11.5%,10种磺胺类药物最低检出浓度为0.01 mg/g.结论:以HPLC法测定鸡肉中10种磺胺类药物残留.操作简便、定量准确可靠.