학술논문

REMOTE DISSOLUTION AND ANALYTICAL PROGRAM FOR IRRADIATED THORIUM
Document Type
Technical Report
Author
Source
Other Information: Orig. Receipt Date: 31-DEC-61
Subject
CHEMISTRY ALUMINUM
CERIUM
CESIUM
CHEMICAL REACTIONS
HYDROFLUORIC ACID
IRRADIATION
ISOTOPES
JACKETS
MEASURED VALUES
MERCURY NITRATES
NITRIC ACID
REMOTE CONTROL
REMOTE HANDLING
SAMPLING
SOLUTIONS
THORIUM
URANIUM
WEIGHT
Language
English
Abstract
A remote dissolution and analytical program for irradiated thorium is given. The aluminum jacket on the slug was dissolved with 6M nitric acid and 0.005M mercuric nitrate. After a water wash, the thorium dissolution was accomplished with concentrated nitric acid made 0.04M in hydrofluoric acid. Weighing, dissolving, and sampling were done remotely in the multicurie cell at the Idaho Chemical Processing Plant. Handling techniques for weighing and dissolving the slugs are described. Transferring and sampling apparatus as well as sampling techniques for the dissolved material are discussed. Analytical data obtained are tabulated. Abstracts of analytical methods for uranium concentration and isotope ratio, aluminum, thorium, cesium, and cerium are given. (auth)