학술논문

Rapid synthesis of indium phosphide
Document Type
Technical Report
Author
Source
Subject
36 MATERIALS SCIENCE INDIUM PHOSPHIDES
SYNTHESIS
BAFFLES
HEAT PIPES
HIGH PRESSURE
STABILITY
TEMPERATURE CONTROL
CONTROL
CONTROL EQUIPMENT
EQUIPMENT
FLOW REGULATORS
INDIUM COMPOUNDS
PHOSPHIDES
PHOSPHORUS COMPOUNDS
PNICTIDES 360601* -- Other Materials-- Preparation & Manufacture
Language
English
Abstract
A method for the high-pressure synthesis (440 psi) of InP is investigated. Independent temperature control of a three-zone furnace incorporating a heat pipe provides a stable temperature profile throughout the synthesis cycle. Internal/external pressure control of the quartz ampoule is maintained by use of a water-cooled baffle and a temperature/pressure balancing program. Complete synthesis is achieved in less than 5 h.