학술논문

Silver nanoparticle thin films deposited on glass surface using an ionic silsesquioxane as stabilizer and as crosslinking agent
Document Type
article
Source
Journal of the Brazilian Chemical Society. May 2015 26(5)
Subject
sol-gel hybrid materials
charged organosilane
thin films
antimicrobial activity
Language
English
ISSN
0103-5053
Abstract
Thin films containing silver nanoparticles homogeneously dispersed, with narrow size distribution below 10 nm, were synthesized on flat glass surface, by using an ionic silsesquioxane as stabilizer and crosslinking agent. The films can be prepared without previous functionalization of substrate surfaces and without addition of other components. The films were heat treated up to 200 ºC and characterized by ultraviolet-visible, transmission electron microscopy, atomic force microscopy, thermogravimetric analysis and ellipsometry. The films were thermally stable when heated up to 200 ºC, presenting the same thickness, and maintaining both optical and morphological properties of silver nanoparticles. The antibacterial activity of the films, containing the silver nanoparticles, was evaluated against Staphylococcus aureus by using the film applicator coating method, showing an excellent performance even after the third cycle of sterilization.