학술논문

Graphene Stress Transducer-Based Thermo-Mechanically Fractured Micro Valve
Document Type
Periodical
Source
Journal of Microelectromechanical Systems J. Microelectromech. Syst. Microelectromechanical Systems, Journal of. 27(3):555-569 Jun, 2018
Subject
Engineered Materials, Dielectrics and Plasmas
Components, Circuits, Devices and Systems
Valves
Heating systems
Graphene
Metals
Polymers
Substrates
Electrodes
Microvalves
thermomechanical processes
microactuators
Language
ISSN
1057-7157
1941-0158
Abstract
This paper presents the design, analysis, and testing of a single-shot thermo-mechanically triggered micromachined micro-valve with graphene on a silicon nitride (Si x N y ) membrane. The graphene serves as a 2-D resistive heater for producing thermo-mechanical stress, to fracture the bilayer formed between nitride and the nickel used to make electrodes. It is demonstrated that the ability of graphene to carry much higher current density per unit than metal heaters enables high thermo-mechanical stress to be generated. The valve is demonstrated as an enabling component of polymer substrate-based vaporizable electronics. It is used for sealing rubidium (Rb) in polymer chambers, and then triggering and exposing it to ambient air to produce heat by exothermic oxidation. This heat energy is used to vaporize the polymers. The nominal valve tested in this work is a $750\,\,\mu \text{m}\,\,\times 750\,\,\mu \text{m}$ membrane of Si x N y . An analytical and finite-element model are presented for the valve, which agree with measured membrane peak-to-peak deflection of $4.1~\mu \text{m}$ just before fracturing, and a peak fracture stress of 395 MPa. The pulsed-power for triggering the valve is nominally 142.1 ± 13.5 mW with a trigger time of 15.4 ± 3.9 ms, resulting in a very low input trigger energy of 2.2 mJ. This trigger energy is $100\times $ lower compared with that of previously reported single-use valves in the literature. [2017–0317]