학술논문

Investigation of the Kinetics of the SHS Process, Initiated Using Electron-Beam Technology
Document Type
Conference
Source
2020 7th International Congress on Energy Fluxes and Radiation Effects (EFRE) Energy Fluxes and Radiation Effects (EFRE), 2020 7th International Congress on. :1118-1124 Sep, 2020
Subject
Components, Circuits, Devices and Systems
Computing and Processing
Engineered Materials, Dielectrics and Plasmas
Engineering Profession
Fields, Waves and Electromagnetics
Power, Energy and Industry Applications
Waveguide transitions
Wires
Process control
Electromagnetic waveguides
Intermetallic
Monitoring
Surface treatment
electron beam
flexible waveguide
monitoring
SHS reaction
vibroacoustic signal
Language
Abstract
The duration of SHS processes occurring in thin films or in near-surface layers of the product is several tens of milliseconds. Under these conditions, the effectiveness of monitoring the reaction of the formation of a new phase can ensured if there is a monitoring system that can build based on processing acoustic emission signals that have shown high sensitivity to transformations occurring in the surface layers of the material. However, a flexible system supplemented with a waveguide which can change its dynamic characteristics and amplitude-frequency response. Experiments have shown that using a wire with a cross-section of up to 2.5 mm 2 as flexible waveguides allows reliable control of vibroacoustic processes in a vacuum chamber at frequencies up to 40 kHz at a distance of more than 2 meters without pre-tensioning. The influence of compaction when removing a conductor of sufficient cross-section from the vacuum chamber insignificantly worsens the values of the transmission coefficients. The article discusses the work of such a system, for example, of monitoring the formation of intermetallic compounds when exposed to pulse low-energy high-current electron beam on the plate of aluminum coated with a thin film of a heat-resistant Nickel alloy. Thanks to the analysis of vibroacoustic signals, it is possible to see how the exothermic chemical reaction proceeds, when the signal character changes. The clusters of points are formed on the graphs, distinguishable in the corresponding coordinates.