학술논문

Morphology and Microstructure Properties of Nanozeolite Coating on Iron Foam With Variation of Calcination Temperature and Chitosan
Document Type
article
Source
Rekayasa Mesin, Vol 12, Iss 3, Pp 561-571 (2022)
Subject
nanozeolite
iron foam
chitosan
morphology
microstructure properties
sem-eds
xrd characterization
Mechanical engineering and machinery
TJ1-1570
Language
English
Indonesian
ISSN
2338-1663
2477-6041
Abstract
Porous materials are widely used in various applications such as ion exchange, separation, drug delivery sensor and water filter application. However porous iron is susceptible to corrosion, therefore coating with corrosion resistant materials is requirede.g. with nanozeolite material. For the application as filter, nanozeolite improves the activities characteristic of iron foam surface since it can act as the agent of ion exchangers and absorb heavy metal ions in water. In the present study, porous metal was coated with nanozeolite by sol-gel coating method. Chitosan concentrations and calcination temperatures are the variable parameter to be optimized in the present research. The mass change of the sample decreases as the chitosan addition increases. The mass change also decreases as the calcination temperature increases. The highest mass change occurs for sample 1 at 14.63%. The morphology of nanozeolite layer showed that the addition of chitosan can decrease the agglomeration of nanozeolite coating. The higher of calcination temperature can homogenize the nanozeolite layer. The particle form of nanozeolite through SEM revealed needle-like, rod and spherical shape. The addition of chitosan can decrease the cluster of nanozeolite particle and the higher of calcination temperature make them more uniform after calcination process. The XRD characterization of sample 5 showed that the nanozeolite particle in this sample was amorphous.