학술논문
藏药阿如久巴丸质量标准研究 / Study on the Quality Standard of Zang Medicine Arujiuba pills
Document Type
Academic Journal
Author
Source
中国民族民间医药 / Chinese Journal of Ethnomedicine and Ethnopharmacy. 33(2):46-50
Subject
Language
Chinese
ISSN
1007-8517
Abstract
目的:修订提高阿如久巴丸的质量标准.方法:参照《中国药典》2020版四部通用检测方法分别测定了阿如久巴丸的水分、总灰分、酸不溶性灰分、浸出物;采用薄层色谱法(TLC)对阿如久巴丸中诃子、红花进行定性鉴别.结果:阿如久巴丸中诃子、红花的薄层色谱斑点清晰,分离度好;阿如久巴丸药材的水分含量平均值为6.99％;阿如久巴丸的总灰分含量平均值为21.43％,建议总灰分不得过26.0％,酸不溶性灰分平均含量为0.296％,建议酸不溶性灰分不得过0.36％;浸出物含量平均值为33.35％,建议浸出物含量不得少于27.0％.结论:所建立的方法操作简便、结果准确,能够用于阿如久巴丸的质量控制.
Objective Revise and improve the quality standard of Arujiuba Pills.Methods The moisture,total ash,acid insolu-ble ash and leachate of Arujiuba Pills were determined according to the four general test methods of the Chinese Pharmacopoeia 2020 e-dition;Qualitative identification of chebula and saffron in Arujiuba Pills by thin layer chromatography(TLC).Results Thin-layer chromatography of chebula and saffron in Arujiuba Pills has clear spots and good separation;The average moisture content of the Aruji-uba Pills was 6.99％;The average total ash content of Arujiuba Pills is 21.43％and it is recommended that the total ash content should not exceed 26.00％;The average acid insoluble ash content was 0.296％and it is recommended that the acid insoluble ash content should not exceed 0.36％;The average leachate content was 33.35％and it is recommended that the leachate content should not be less than 27.0％.Conclusion The method developed is simple to operate,accurate and can be used for quality control of Aru-jiuba Pills.
Objective Revise and improve the quality standard of Arujiuba Pills.Methods The moisture,total ash,acid insolu-ble ash and leachate of Arujiuba Pills were determined according to the four general test methods of the Chinese Pharmacopoeia 2020 e-dition;Qualitative identification of chebula and saffron in Arujiuba Pills by thin layer chromatography(TLC).Results Thin-layer chromatography of chebula and saffron in Arujiuba Pills has clear spots and good separation;The average moisture content of the Aruji-uba Pills was 6.99％;The average total ash content of Arujiuba Pills is 21.43％and it is recommended that the total ash content should not exceed 26.00％;The average acid insoluble ash content was 0.296％and it is recommended that the acid insoluble ash content should not exceed 0.36％;The average leachate content was 33.35％and it is recommended that the leachate content should not be less than 27.0％.Conclusion The method developed is simple to operate,accurate and can be used for quality control of Aru-jiuba Pills.