학술논문

Synthesis and properties of methyl hydropyrimidineacetates.
Document Type
Article
Source
Chemistry of Heterocyclic Compounds. Jul2007, Vol. 43 Issue 7, p926-935. 10p. 1 Diagram, 6 Charts, 1 Graph.
Subject
*SPECTRUM analysis
*CHEMICAL reactions
*HYDROCARBONS
*MASS (Physics)
*NUCLEAR spectroscopy
*MASS spectrometry
*PHENYLENEDIAMINES
Language
ISSN
0009-3122
Abstract
The alkylation of 1-aryl-substituted dihydro-2,4(1H,3H)-pyrimidinediones with methyl 2-bromoacetate has been studied followed by hydrolysis and condensation of the products with o-phenylenediamine. The compounds have been identified by NMR, and IR spectrometry and mass spectrometry. Structural characteristics in the 1H and 13C NMR spectra of the synthesized are discussed. [ABSTRACT FROM AUTHOR]