학술논문

A Combined Raman Spectroscopy and Atomic Force Microscopy System for In Situ and Real-Time Measures in Electrochemical Cells.
Document Type
Article
Source
Materials (1996-1944). Mar2023, Vol. 16 Issue 6, p2239. 10p.
Subject
*ATOMIC spectroscopy
*ATOMIC force microscopy
*ELECTRIC batteries
*RAMAN spectroscopy
*ANALYTICAL chemistry
Language
ISSN
1996-1944
Abstract
An innovative and versatile set-up for in situ and real time measures in an electrochemical cell is described. An original coupling between micro-Raman spectroscopy and atomic force microscopy enables one to collect data on opaque electrodes. This system allows for the correlation of topographic images with chemical maps during the charge exchange occurring in oxidation/reduction processes. The proposed set-up plays a crucial role when reactions, both reversible and non-reversible, are studied step by step during electrochemical reactions and/or when local chemical analysis is required. [ABSTRACT FROM AUTHOR]