학술논문

A combined ion-sputtering and electron-beam annealing device for the in vacuo postpreparation of scanning probes.
Document Type
Article
Source
Review of Scientific Instruments. Mar2011, Vol. 82 Issue 3, p033701. 4p. 1 Color Photograph, 2 Black and White Photographs, 1 Diagram, 1 Graph.
Subject
*SCANNING tunneling microscopy
*SPUTTERING (Physics)
*ELECTRON beams
*SCANNING probe microscopy
*ULTRAHIGH vacuum
*X-ray spectroscopy
*ELECTROCHEMISTRY
Language
ISSN
0034-6748
Abstract
We describe the setup, characteristics, and application of an in vacuo ion-sputtering and electron-beam annealing device for the postpreparation of scanning probes (e.g., scanning tunneling microscopy (STM) tips) under ultrahigh vacuum (UHV) conditions. The proposed device facilitates the straightforward implementation of a common two-step cleaning procedure, where the first step consists of ion-sputtering, while the second step heals out sputtering-induced defects by thermal annealing. In contrast to the standard way, no dedicated external ion-sputtering gun is required with the proposed device. The performance of the described device is demonstrated by SEM micrographs and energy dispersive x-ray characterization of electrochemically etched tungsten tips prior and after postprocessing. [ABSTRACT FROM AUTHOR]