학술논문

Microstructural investigation of PBX 9501: Comparing wet slurry and resonant acoustic mixing techniques.
Document Type
Article
Source
AIP Conference Proceedings. 2023, Vol. 2844 Issue 1, p1-5. 5p.
Subject
*SMALL-angle X-ray scattering
*SLURRY
*PARTICLE size distribution
*X-ray scattering
Language
ISSN
0094-243X
Abstract
The microstructure of a high explosive (HE) material directly influences the reactive behavior under a variety of insults. Furthermore, the preparation method of polymer-bonded explosives (PBX), as well as the constituent material particle size distribution and consolidation parameters, will dominate the microstructural features that are observed. Here, we compare batches of PBX 9501 prepared by the typical wet slurry process and those prepared by resonant acoustic mixing. The "prills" produced by the wet slurry process leads to an inherently different microstructure than the coated powder produced by resonant acoustic mixing. We observed that the conditions required to consolidate (press) the material to the nominal PBX 9501 density varied depending on the preparation technique, which also dictates the observed binder distribution. Furthermore, X-ray microcomputed tomography and ultra-small-angle X-ray scattering analyses revealed distinct differences in the void structure and distribution. [ABSTRACT FROM AUTHOR]