학술논문

Repeatability and reproducibility of measurements of low dissolved radiocesium concentrations in freshwater using different pre-concentration methods.
Document Type
Article
Source
Journal of Radioanalytical & Nuclear Chemistry. Nov2019, Vol. 322 Issue 2, p477-485. 9p. 3 Diagrams, 1 Chart, 1 Graph.
Subject
*STATISTICAL reliability
*SOLID phase extraction
*CESIUM
*STANDARD deviations
*CESIUM ions
*FRESH water
*STATISTICAL accuracy
*MEASUREMENT
Language
ISSN
0236-5731
Abstract
We assessed the repeatability and reproducibility of methods for determining low dissolved radiocesium concentrations in freshwater in Fukushima. Twenty-one laboratories pre-concentrated three of 10 L samples by five different pre-concentration methods (Prussian-blue-impregnated filter cartridges, coprecipitation with ammonium phosphomolybdate, evaporation, solid-phase extraction disks, and ion-exchange resin columns), and activity of radiocesium was measured. The z-scores for all of the 137Cs results were within ± 2, indicating that the methods were a good degree of precision. The relative standard deviations (RSDs) indicating the reproducibility among different laboratories were larger than the RSDs indicating the repeatability in each separate laboratory. [ABSTRACT FROM AUTHOR]