학술논문
N , N ′-Dipropyloxamide.
Document Type
Article
Author
Source
Subject
*MELTING points
*SINGLE crystals
*HYDROGEN bonding
*METHANOL
*CRYSTAL structure
*NUCLEAR magnetic resonance spectroscopy
*ETHANOL
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Language
ISSN
1422-8599
Abstract
N,N′-Dipropyloxamide (1) was synthesised by the reaction between diethyloxalate and n-propylamine in ethanol. Compound 1 was fully characterised by both microanalytical (elemental analysis, melting point determination) and spectroscopic means (FT-IR and NMR spectroscopy). Crystals suitable for single crystal X-ray diffraction were isolated by the slow evaporation of a methyl alcohol solution of the compound. The resulting crystal structure shows the prominent role exerted by intermolecular hydrogen bonds in the crystal packing. [ABSTRACT FROM AUTHOR]