학술논문

ATR microreactor: A tool for in-situ and spatial reaction monitoring
Document Type
Conference
Source
2022 IEEE Sensors Sensors, 2022 IEEE. :1-4 Oct, 2022
Subject
Engineering Profession
General Topics for Engineers
Spectroscopy
Sensor phenomena and characterization
Position measurement
Chemical reactions
Reflection
Time measurement
Nanoscale devices
nanofabrication
microreactor
mixers
insitu reaction monitoring
Language
ISSN
2168-9229
Abstract
We report the fabrication of a microreactor with embedded internal reflection element (IRE) and herringbone (HB) micromixer. The microreactor can be used as a powerful tool for monitoring in-situ chemical reactions when combined with attenuated total internal reflection (ATR) infrared (IR) spectroscopy. In this work, a H 2 O/D 2 O model reaction was monitored as a proof of concept and the HOD product formation was spatially tracked. In addition to this, a mixing efficiency of 99% at 25 cycles was also calculated for the microreactor.