학술논문

New frontiers in atom probe tomography: a review of research enabled by cryo and/or vacuum transfer systems
Document Type
article
Source
Materials Today Advances, Vol 7, Iss , Pp 100090- (2020)
Subject
Focused ion beam
Catalysis
Hydrogen
Deuterium
Organic
Cryogenic
Materials of engineering and construction. Mechanics of materials
TA401-492
Language
English
ISSN
2590-0498
Abstract
There has been a recent surge in the use of cryo and/or vacuum specimen preparation and transfer systems to broaden the scope of research enabled by the microscopy technique of atom probe tomography. This is driven by the fact that, as for many microscopes, the application of atom probes to air- and temperature-sensitive materials or wet biological specimens has previously been limited by transfer through air at room temperature. Here we provide an overview of areas of research that benefit from these new transfer and analysis protocols, as well as a review of current advances in transfer devices, environmental cells, and glove boxes for controlled specimen manipulation. This includes the study of catalysis and corrosion, biological samples, liquid-solid interfaces, natural aging, and the distribution of hydrogen in materials.