학술논문

Optimal bias voltage of substrate for formable nanocrystalline Niobium precoatings of metallic bipolar plates
Document Type
Conference
Source
2022 8th International Conference on Nanomanufacturing & 4th AET Symposium on ACSM and Digital Manufacturing (Nanoman-AETS) Nanomanufacturing & 4th AET Symposium on ACSM and Digital Manufacturing (Nanoman-AETS), 2022 8th International Conference on. :1-6 Aug, 2022
Subject
Aerospace
Bioengineering
Components, Circuits, Devices and Systems
Engineered Materials, Dielectrics and Plasmas
Photonics and Electrooptics
Robotics and Control Systems
Surface morphology
Ions
Manufacturing
Coatings
Voltage control
Substrates
Niobium
Metallic bipolar plates
Niobium precoatings
Bias voltage of substrate
Micro-forming
Coating fracture
Nanocrystalline
Language
Abstract
Metallic bipolar plates (BPPs) are key components of the proton exchange membrane fuel cells. To further improve the manufacturing efficiency of metallic BPPs, precoatings have attracted much attention recently. However, precoatings tend to crack and loss the integrity during the forming process. Therefore, formable precoatings are in great demand, and the relationship between deposition and formability of precoatings needs to be studied. In this research, Niobium (Nb) precoatings with different bias voltages of substrate are deposited on SS316L with unbalanced magnetron sputtering process. To evaluate the formability, uniaxial tensile tests are conducted. As the bias voltage increases, the formability of the precoatings firstly increases and reaches the maximum when the bias voltage is −60 V. With further increase of bias voltage, the formability is deteriorated. To understand the effect of bias voltage, the microstructure and surface morphology of the samples are characterized. Nb precoatings with great compactness and nanocrystalline state can sustain 30 % engineering strain when the bias voltage is −60 V, which is the optimal bias voltage for formable Nb precoatings.